The milling of FBCC was performed using a planetary micromill Pulverisette7 (Fritsch , Germany). The milling was carried out using distilled water, in three cycles, each cycle consisting of a milling phase of 30 min and a 30-min break. After the milling, the samples were dried at 110 °C. The FBCC samples were burnt for 5 h at 1200 …
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